6 Aluminum Lake 50 None 75. FD C Blue No. 2 Aluminum Lake, FD C Red No. 40 Aluminum Lake 88 D C Yellow No. 10 Aluminum Lake, FD C Blue No.
Procedure Separately inject equal volumes (about 100 L) of the Standard preparation and the Assay preparation into the chromatograph, record the chromatograms, and measure the responses for the major peaks. Calculate the percentage of C 15 H 10 I 4 NNaO 4 in the portion of Levothyroxine Sodium taken by the formula: 100 C S.
Before having surgery, tell your doctor or dentist about all the products you use (including prescription drugs, nonprescription drugs, and herbal products). Current information shows that this drug may be used during pregnancy.
Contraindications Levothyroxine sodium tablets are contraindicated in patients with untreated subclinical (suppressed serum TSH level with normal T 3 and T 4 levels) or overt thyrotoxicosis of any etiology and in patients with acute myocardial infarction.
Levothyroxine stock solution Dissolve an accurately weighed quantity of USP Levothyroxine RS in 0.01 M Methanolic sodium hydroxide to obtain a solution having a known concentration of about 0.4 mg of levothyroxine per mL.
Chromatographic system (see Chromatography 621 ) The liquid chromatograph is equipped with a 225-nm detector and a 4.6-mm 25-cm column that contains packing L10. The flow rate is about 1.5 mL per minute.
Pituitary TSH Suppression In the treatment or prevention of various types of euthyroid goiters (see WARNINGS and PRECAUTIONS including thyroid nodules (see WARNINGS and PRECAUTIONS subacute or chronic lymphocytic thyroiditis (Hashimotos thyroiditis multinodular goiter (see WARNINGS and PRECAUTIONS ) and, as an adjunct to surgery and radioiodine therapy in the management of thyrotropin-dependent well differentiated.
1 Aluminum Lake, FD C Yellow No. 6 Aluminum Lake 100 D C Yellow No. 10 Aluminum Lake, FD C Yellow No. 6 Aluminum Lake 112 D C Red No. 27 Aluminum Lake, D C Red No.
This product may contain inactive ingredients, which can cause allergic reactions or other problems. Talk to your pharmacist for more details. Before using this medication, tell your doctor or pharmacist your medical history, especially of: increased thyroid hormones (thyrotoxicosis decreased adrenal gland function, heart disease (such as coronary artery disease, irregular heartbeat high blood pressure.
Make a 1:100 dilution of this solution using Mobile phase. Standard preparation Transfer appropriate volumes of Levothyroxine stock solution and Liothyronine stock solution to a suitable container, and dilute quantitatively and stepwise, if necessary, with Mobile phase to obtain a solution having known concentrations of about 10 g of levothyroxine per mL and 0.2 g.
Assay preparation Transfer an accurately weighed portion of about 100 g of Levothyroxine Sodium into a centrifuge tube, add 2 glass beads, pipet 10 mL of Mobile phase into the tube, and mix using a vortex mixer for 3 minutes.
30 Aluminum Lake 125 FD C Blue No. 1 Aluminum Lake, FD C Red No. 40 Aluminum Lake, FD C Yellow No. 6 Aluminum Lake 137 FD C Blue No. 2 Aluminum Lake 150 FD C Blue No.
Limit of inorganic iodides Extracting solution. Prepare a 1 in 100 solution of sulfuric acid in water. Reference solution Dissolve an accurately weighed quantity of potassium iodide in water to obtain a stock solution containing 0.131 mg, equivalent to 0.100 mg of iodide per mL.
33(3) Page 422 Chromatographic Column Chromatographic columns text is not derived from, and not part of, USP 32 or NF 27.
Auxiliary Information Please check for your question in the FAQs before contacting USP. Topic/Question Contact Expert Committee Monograph Elena Gonikberg, Ph. D. Senior Scientist (MDGRE 05) Monograph Development-Gastrointestinal Renal and Endocrine Reference Standards Lili Wang, Technical Services Scientist USP32NF Pharmacopeial Forum : Volume No.